Semi Batch Reactor An isothermal semi-cluster reactor is a semi-shut framework with one information stream. It is worked under conditions like Isothermal (Temperature of Reaction Mass stays consistent) and consummately blended (arrangement of response blend is uniform all through). This set-up is utilized to think about a non-synergist homogeneous response under isothermal condition. The set up comprises of a Reactor fitted in a steady temperature water shower. Before beginning the response the reactor is accused of estimated amount of one reactant. From a nourish tank another reactant is encouraged to the reactor. Utilizing an inspecting pipette tests can be taken out for investigation after settled interim. Rotameter is given to gauge the stream of Chemicals. The packed air is utilized for course of nourish. One stirrer is fitted for blending the reactants in reactor and other is fitted in water shower to keep the uniform temperature all through in the shower. The temperature of shower can be kept up from encompassing to 70C with the assistance of Digital Temperature pointer Cum Controller. Weight Regulator, Pressure Gauge and Safety Valve are fitted in the compacted carrier. EXPERIMENTATION: To think about a moment arrange sponification response in a Semi-Batch Reactor. To decide the Reaction Rate Constant. UTILITIES REQUIRED : Compressed Air Supply at 2 Bar, 0.25 CFM. Water supply and deplete. Power 1.5kw, Single. Instruments, Laboratory products and Chemicals required for examination according to the framework embraced. Specialized DETAILS : QQ Reactor : Material Stainless Steel, Capacity 3 Ltrs. (approx). QQ Water Bath : Material Stainless Steel, Double divider, protected with Ceramic Wool. QQ Heater : Nichrome wire Heater QQ Stirrer : Material Stainless Steel Impeller and shaft combined with FHP engine QQ Feed Tank (1Nos.) : Material Stainless Steel, Capacity - 20 Ltrs. QQ Feed Circulation : By compacted air. QQ Flow Measurement : Rotameter. QQ Piping : Material Stainless Steel and PVC. QQ Pressure Regulator : 0-2 Kg/cm2 QQ Pressure Gauge : Bourdon compose 0-2 Kg/cm2 .
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